TA Instruments

AR1755-0003f

15/03/2013 14:37:14

Sample name	ASW Blank coupon#20 + DI + beads 
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1755
Run number	3 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:37:14

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 50.00 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	49.99	-658.54	10000	20.0	0.1536	1.008	-214.7	62.49	-3.435	625.8	45.0455	0.1603	56.307	5630.7	3.411E-3	0.0	0.0
2.0240	50.00	36.607	10000	20.0	0.1534	2.024	11.93	62.49	0.1909	625.0	95.2676	0.1600	119.08	11908	3.411E-3	0.0	0.0
3.0240	50.00	36.580	10000	20.0	0.1552	3.024	11.92	62.50	0.1908	632.4	145.8570	0.1619	182.32	18232	3.411E-3	0.1	0.1
4.0080	50.00	36.460	10000	20.0	0.1548	4.008	11.88	62.50	0.1901	630.7	195.8330	0.1615	244.79	24479	3.411E-3	0.1	0.1
5.0080	50.00	36.321	10000	20.0	0.1524	5.008	11.84	62.50	0.1894	620.8	246.0990	0.1589	307.62	30762	3.411E-3	0.1	0.1
6.0080	50.00	36.735	10000	20.0	0.1534	6.008	11.97	62.50	0.1916	625.0	296.5210	0.1600	370.65	37065	3.411E-3	0.1	0.1
7.0080	50.00	36.078	10000	20.0	0.1540	7.008	11.76	62.50	0.1882	627.4	346.9590	0.1606	433.70	43370	3.411E-3	0.1	0.1
8.0080	50.00	35.947	10000	20.0	0.1522	8.008	11.72	62.50	0.1875	620.0	396.8850	0.1587	496.11	49611	3.411E-3	0.1	0.1
9.0240	50.00	36.024	10000	20.0	0.1512	9.024	11.74	62.50	0.1879	615.9	447.1410	0.1577	558.93	55893	3.411E-3	0.2	0.2
10.008	50.00	36.228	10000	20.0	0.1524	10.008	11.81	62.50	0.1889	620.8	497.4030	0.1589	621.75	62175	3.411E-3	0.2	0.2
11.008	50.00	36.147	10000	20.0	0.1536	11.008	11.78	62.50	0.1885	625.8	547.6790	0.1602	684.60	68460	3.411E-3	0.2	0.2
12.012	50.00	36.036	10000	20.0	0.1503	12.012	11.75	62.50	0.1879	612.5	597.9540	0.1568	747.44	74744	3.411E-3	0.2	0.2
13.016	50.00	35.778	10000	20.0	0.1514	13.016	11.66	62.50	0.1866	616.7	648.2230	0.1579	810.28	81028	3.411E-3	0.2	0.2
14.024	50.00	35.585	10000	20.0	0.1522	14.024	11.60	62.50	0.1856	620.0	698.4850	0.1587	873.11	87311	3.411E-3	0.2	0.2
15.008	50.00	35.827	10000	20.0	0.1499	15.008	11.68	62.50	0.1868	610.9	748.9330	0.1564	936.17	93617	3.411E-3	0.3	0.3
16.008	50.00	35.396	10000	20.0	0.1528	16.008	11.54	62.50	0.1846	622.5	799.0100	0.1593	998.76	99876	3.411E-3	0.3	0.3
17.012	50.00	35.834	10000	20.0	0.1514	17.012	11.68	62.50	0.1869	616.7	849.7330	0.1579	1062.2	1.0622E5	3.411E-3	0.3	0.3
18.008	50.00	36.000	10000	20.0	0.1528	18.008	11.73	62.50	0.1877	622.5	899.8170	0.1594	1124.8	1.1248E5	3.411E-3	0.3	0.3
19.008	50.00	36.137	10000	20.0	0.1524	19.008	11.78	62.50	0.1885	620.8	950.1040	0.1589	1187.6	1.1876E5	3.411E-3	0.3	0.3
20.024	50.00	35.542	10000	20.0	0.1528	20.024	11.58	62.50	0.1854	622.5	1000.3200	0.1594	1250.4	1.2504E5	3.411E-3	0.3	0.3
21.024	50.00	35.590	10000	20.0	0.1548	21.024	11.60	62.50	0.1856	630.7	1050.8000	0.1615	1313.5	1.3135E5	3.411E-3	0.4	0.4
22.008	50.00	35.971	10000	20.0	0.1516	22.008	11.72	62.50	0.1876	617.5	1075.5699	0.1581	1344.5	1.3445E5	3.411E-3	0.4	0.4
23.008	50.00	35.632	10000	20.0	0.1530	23.008	11.61	62.50	0.1858	623.3	1125.7400	0.1596	1407.2	1.4072E5	3.411E-3	0.4	0.4
24.008	50.00	35.567	10000	20.0	0.1538	24.008	11.59	62.50	0.1855	626.6	1176.0300	0.1604	1470.0	1.4700E5	3.411E-3	0.4	0.4
25.008	50.00	36.018	10000	20.0	0.1524	25.008	11.74	62.50	0.1878	620.8	1226.2800	0.1589	1532.9	1.5329E5	3.411E-3	0.4	0.4
26.012	50.00	35.795	10000	20.0	0.1544	26.012	11.67	62.50	0.1867	629.1	1276.5500	0.1610	1595.7	1.5957E5	3.411E-3	0.4	0.4
27.008	50.00	35.595	10000	20.0	0.1526	27.008	11.60	62.50	0.1856	621.6	1326.8199	0.1591	1658.5	1.6585E5	3.411E-3	0.5	0.5
28.008	50.00	35.478	10000	20.0	0.1530	28.008	11.56	62.50	0.1850	623.3	1377.2100	0.1596	1721.5	1.7215E5	3.411E-3	0.5	0.5
29.008	50.00	35.558	10000	20.0	0.1546	29.008	11.59	62.50	0.1854	629.9	1427.3101	0.1613	1784.1	1.7841E5	3.411E-3	0.5	0.5
30.024	50.00	35.704	10000	20.0	0.1534	30.024	11.64	62.50	0.1862	625.0	1478.9100	0.1600	1848.6	1.8486E5	3.411E-3	0.5	0.5
31.024	50.00	35.702	10000	20.0	0.1544	31.024	11.64	62.50	0.1862	629.1	1529.0000	0.1610	1911.3	1.9113E5	3.411E-3	0.5	0.5
32.008	50.00	36.282	10000	20.0	0.1510	32.008	11.83	62.50	0.1892	615.0	1578.1500	0.1574	1972.7	1.9727E5	3.411E-3	0.5	0.5
33.008	50.00	36.099	10000	20.0	0.1536	33.008	11.77	62.50	0.1883	625.8	1628.4600	0.1602	2035.6	2.0356E5	3.411E-3	0.6	0.6
34.024	50.00	35.912	10000	20.0	0.1516	34.024	11.71	62.50	0.1873	617.5	1678.7800	0.1581	2098.5	2.0985E5	3.411E-3	0.6	0.6
35.008	50.00	35.527	10000	20.0	0.1495	35.008	11.58	62.50	0.1853	609.2	1728.9200	0.1560	2161.2	2.1612E5	3.411E-3	0.6	0.6
36.024	50.00	35.799	10000	20.0	0.1524	36.024	11.67	62.50	0.1867	620.8	1779.1801	0.1589	2224.0	2.2240E5	3.411E-3	0.6	0.6
37.008	50.00	35.786	10000	20.0	0.1546	37.008	11.66	62.50	0.1866	629.9	1829.4500	0.1613	2286.8	2.2868E5	3.411E-3	0.6	0.6
38.008	50.00	35.970	10000	20.0	0.1516	38.008	11.72	62.50	0.1876	617.5	1879.8000	0.1581	2349.8	2.3498E5	3.411E-3	0.6	0.6
39.024	50.00	35.813	10000	20.0	0.1520	39.024	11.67	62.50	0.1868	619.2	1930.0000	0.1585	2412.5	2.4125E5	3.411E-3	0.7	0.7
40.008	50.00	35.693	10000	20.0	0.1516	40.008	11.63	62.50	0.1861	617.5	1980.6300	0.1581	2475.8	2.4758E5	3.411E-3	0.7	0.7
41.008	50.00	35.794	10000	20.0	0.1505	41.008	11.67	62.50	0.1867	613.4	2030.5300	0.1570	2538.2	2.5382E5	3.411E-3	0.7	0.7
42.008	50.00	35.293	10000	20.0	0.1536	42.008	11.50	62.50	0.1841	625.8	2080.7900	0.1602	2601.0	2.6010E5	3.411E-3	0.7	0.7
43.008	50.00	35.445	10000	20.0	0.1536	43.008	11.55	62.50	0.1849	625.8	2131.2800	0.1602	2664.1	2.6641E5	3.411E-3	0.7	0.7
44.020	50.00	35.445	10000	20.0	0.1524	44.020	11.55	62.50	0.1848	620.8	2181.3201	0.1589	2726.7	2.7267E5	3.411E-3	0.7	0.7
45.008	50.00	35.878	10000	20.0	0.1491	45.008	11.69	62.50	0.1871	607.6	2231.5701	0.1555	2789.5	2.7895E5	3.411E-3	0.8	0.8
46.008	50.00	35.964	10000	20.0	0.1505	46.008	11.72	62.50	0.1876	613.4	2281.8501	0.1570	2852.3	2.8523E5	3.411E-3	0.8	0.8
47.024	50.00	35.866	10000	20.0	0.1501	47.024	11.69	62.50	0.1870	611.7	2332.3201	0.1566	2915.4	2.9154E5	3.411E-3	0.8	0.8
48.020	50.00	35.208	10000	20.0	0.1503	48.020	11.48	62.50	0.1836	612.5	2382.5901	0.1568	2978.2	2.9782E5	3.411E-3	0.8	0.8
49.020	50.00	35.785	10000	20.0	0.1514	49.020	11.66	62.50	0.1866	616.7	2433.1201	0.1579	3041.4	3.0414E5	3.411E-3	0.8	0.8
50.008	50.00	35.696	10000	20.0	0.1512	50.008	11.64	62.50	0.1862	615.9	2483.3501	0.1577	3104.2	3.1042E5	3.411E-3	0.8	0.8
51.008	50.00	35.472	10000	20.0	0.1538	51.008	11.56	62.50	0.1850	626.6	2533.3999	0.1604	3166.8	3.1668E5	3.411E-3	0.9	0.9
52.004	50.00	35.348	10000	20.0	0.1493	52.004	11.52	62.50	0.1843	608.4	2583.7300	0.1558	3229.7	3.2297E5	3.411E-3	0.9	0.9
53.020	50.00	35.388	10000	20.0	0.1510	53.020	11.53	62.50	0.1846	615.0	2633.9099	0.1574	3292.4	3.2924E5	3.411E-3	0.9	0.9
54.008	50.00	35.726	10000	20.0	0.1493	54.008	11.64	62.50	0.1863	608.4	2684.2400	0.1558	3355.3	3.3553E5	3.411E-3	0.9	0.9
55.008	50.00	35.639	10000	20.0	0.1501	55.008	11.62	62.50	0.1859	611.7	2734.4500	0.1566	3418.1	3.4181E5	3.411E-3	0.9	0.9
56.020	50.00	35.327	10000	20.0	0.1481	56.020	11.51	62.50	0.1842	603.5	2784.7500	0.1545	3480.9	3.4809E5	3.411E-3	0.9	0.9
57.020	50.00	35.882	10000	20.0	0.1534	57.020	11.70	62.50	0.1871	625.0	2835.5901	0.1600	3544.5	3.5445E5	3.411E-3	1.0	1.0
58.008	50.00	36.226	10000	20.0	0.1491	58.008	11.81	62.50	0.1889	607.6	2885.4800	0.1555	3606.9	3.6069E5	3.411E-3	1.0	1.0
59.008	50.00	35.904	10000	20.0	0.1514	59.008	11.70	62.50	0.1872	616.7	2935.2900	0.1579	3669.1	3.6691E5	3.411E-3	1.0	1.0
60.008	50.00	35.222	10000	20.0	0.1503	60.008	11.48	62.50	0.1837	612.5	2985.8201	0.1568	3732.3	3.7323E5	3.411E-3	1.0	1.0

